To grind each mixture intensively, a planetary ball mill (Pulverizette7, Fritsch Gmbh, IdarOberstein, Germany) was used. The mill conditions were as follows: 4 g of each mixture was placed into a zirconia pot (45 cm 3 inner volume) with seven 15mm diameter zirconia balls and then was subjected to grinding in air at 700 rpm for various periods of time.
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